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Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides. / Sarkar, Subhankar; Pal, Satyajit; Mukherjee, Anindita et al.
In: Journal of Organic Chemistry, Vol. 89, No. 3, 2024, p. 1473-1482.

Research output: Contribution to journal › Article › peer-review

Harvard

Sarkar, S, Pal, S, Mukherjee, A, Santra, S, Zyryanov, G & Majee, A 2024, 'Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides', Journal of Organic Chemistry, vol. 89, no. 3, pp. 1473-1482. https://doi.org/10.1021/acs.joc.3c02081

APA

Sarkar, S., Pal, S., Mukherjee, A., Santra, S., Zyryanov, G., & Majee, A. (2024). Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides. Journal of Organic Chemistry, 89(3), 1473-1482. https://doi.org/10.1021/acs.joc.3c02081

Vancouver

Sarkar S, Pal S, Mukherjee A, Santra S, Zyryanov G, Majee A. Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides. Journal of Organic Chemistry. 2024;89(3):1473-1482. doi: 10.1021/acs.joc.3c02081

Author

Sarkar, Subhankar ; Pal, Satyajit ; Mukherjee, Anindita et al. / Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides. In: Journal of Organic Chemistry. 2024 ; Vol. 89, No. 3. pp. 1473-1482.

BibTeX

@article{ed7745a5a7df4d289dbe89ebaed3ac2e,
title = "Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides",
abstract = "A convenient and new synthetic approach has been developed for the oxidative cross-coupling of the C-N bond through the reaction between arylglyoxylic acids and tetraalkylthiuram disulfides. The reaction proceeds under ambient air at room temperature in the presence of visible light. This reaction offers a metal-, base-, photocatalyst-, and solvent-free synthesis of various α-ketoamides with moderate to excellent yields via the radical pathway. In addition, this protocol demonstrates the potential application of a gram-scale synthesis. {\textcopyright} 2024 American Chemical Society.",
author = "Subhankar Sarkar and Satyajit Pal and Anindita Mukherjee and Sougata Santra and Grigory Zyryanov and Adinath Majee",
note = "A.M. and S.S. acknowledge financial support from the CSIR-Major Research Project (ref no. 02(0383)/19/EMR-II). The authors are thankful to the DST-FIST and UGC-SAP program of the Department of Chemistry, Visva-Bharati. G.V.Z. and S.S. also acknowledge financial support from the Ministry of Science and Higher Education of the Russian Federation (ref # 075-15-2022-1118 dated 29 June 2022).",
year = "2024",
doi = "10.1021/acs.joc.3c02081",
language = "English",
volume = "89",
pages = "1473--1482",
journal = "Journal of Organic Chemistry",
issn = "0022-3263",
publisher = "American Chemical Society",
number = "3",

}

RIS

TY - JOUR

T1 - Visible-Light-Promoted Metal- and Photocatalyst-Free Reactions between Arylglyoxylic Acids and Tetraalkylthiuram Disulfides: Synthesis of α-Ketoamides

AU - Sarkar, Subhankar

AU - Pal, Satyajit

AU - Mukherjee, Anindita

AU - Santra, Sougata

AU - Zyryanov, Grigory

AU - Majee, Adinath

N1 - A.M. and S.S. acknowledge financial support from the CSIR-Major Research Project (ref no. 02(0383)/19/EMR-II). The authors are thankful to the DST-FIST and UGC-SAP program of the Department of Chemistry, Visva-Bharati. G.V.Z. and S.S. also acknowledge financial support from the Ministry of Science and Higher Education of the Russian Federation (ref # 075-15-2022-1118 dated 29 June 2022).

PY - 2024

Y1 - 2024

N2 - A convenient and new synthetic approach has been developed for the oxidative cross-coupling of the C-N bond through the reaction between arylglyoxylic acids and tetraalkylthiuram disulfides. The reaction proceeds under ambient air at room temperature in the presence of visible light. This reaction offers a metal-, base-, photocatalyst-, and solvent-free synthesis of various α-ketoamides with moderate to excellent yields via the radical pathway. In addition, this protocol demonstrates the potential application of a gram-scale synthesis. © 2024 American Chemical Society.

AB - A convenient and new synthetic approach has been developed for the oxidative cross-coupling of the C-N bond through the reaction between arylglyoxylic acids and tetraalkylthiuram disulfides. The reaction proceeds under ambient air at room temperature in the presence of visible light. This reaction offers a metal-, base-, photocatalyst-, and solvent-free synthesis of various α-ketoamides with moderate to excellent yields via the radical pathway. In addition, this protocol demonstrates the potential application of a gram-scale synthesis. © 2024 American Chemical Society.

UR - http://www.scopus.com/inward/record.url?partnerID=8YFLogxK&scp=85183090985

UR - https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=tsmetrics&SrcApp=tsm_test&DestApp=WOS_CPL&DestLinkType=FullRecord&KeyUT=001157571500001

U2 - 10.1021/acs.joc.3c02081

DO - 10.1021/acs.joc.3c02081

M3 - Article

VL - 89

SP - 1473

EP - 1482

JO - Journal of Organic Chemistry

JF - Journal of Organic Chemistry

SN - 0022-3263

IS - 3

ER -

ID: 52961149