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Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry. / Shtin, T.; Gurvich, V.; Galasheva, O. et al.
In: Inorganic Materials, Vol. 59, No. 14, 01.12.2023, p. 1387-1395.

Research output: Contribution to journal › Article › peer-review

Harvard

Shtin, T, Gurvich, V, Galasheva, O, Shelomentsev, I, Neudachina, L & Shtin, S 2023, 'Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry', Inorganic Materials, vol. 59, no. 14, pp. 1387-1395. https://doi.org/10.1134/S0020168523140133

APA

Shtin, T., Gurvich, V., Galasheva, O., Shelomentsev, I., Neudachina, L., & Shtin, S. (2023). Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry. Inorganic Materials, 59(14), 1387-1395. https://doi.org/10.1134/S0020168523140133

Vancouver

Shtin T, Gurvich V, Galasheva O, Shelomentsev I, Neudachina L, Shtin S. Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry. Inorganic Materials. 2023 Dec 1;59(14):1387-1395. doi: 10.1134/S0020168523140133

Author

Shtin, T. ; Gurvich, V. ; Galasheva, O. et al. / Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry. In: Inorganic Materials. 2023 ; Vol. 59, No. 14. pp. 1387-1395.

BibTeX

@article{653f537149064b039ed0f2740e93d772,
title = "Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry",
abstract = "A method for determination of polyorganosiloxanes (by silicon) in water using high-resolution continuum source electrothermal atomic absorption spectrometry with the preliminary extraction of the analytes from the analyzed sample by benzene is proposed. The parameters of the time–temperature program of an atomizer are optimized using a storm water sample. To eliminate chemical interference during the determination of silicon, graphite cuvettes have been modified with a permanent modifier (sodium tungstate) to form a carbide coating. The thermal stabilization of silicon in a graphite furnace has been achieved in the presence of a mixed palladium–magnesium modifier in the nitrate form. The developed method of analysis has been used to determine the content of polyorganosiloxanes (by silicon) in natural water samples. The metrological characteristics of the method in the determined silicon content range of 0.01–100 mg/dm3 have been estimated.",
author = "T. Shtin and V. Gurvich and O. Galasheva and I. Shelomentsev and L. Neudachina and S. Shtin",
year = "2023",
month = dec,
day = "1",
doi = "10.1134/S0020168523140133",
language = "English",
volume = "59",
pages = "1387--1395",
journal = "Inorganic Materials",
issn = "0020-1685",
publisher = "Maik Nauka-Interperiodica Publishing",
number = "14",

}

RIS

TY - JOUR

T1 - Determination of Polyorganosiloxanes (by Silicon) in Water by Extraction High-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometry

AU - Shtin, T.

AU - Gurvich, V.

AU - Galasheva, O.

AU - Shelomentsev, I.

AU - Neudachina, L.

AU - Shtin, S.

PY - 2023/12/1

Y1 - 2023/12/1

N2 - A method for determination of polyorganosiloxanes (by silicon) in water using high-resolution continuum source electrothermal atomic absorption spectrometry with the preliminary extraction of the analytes from the analyzed sample by benzene is proposed. The parameters of the time–temperature program of an atomizer are optimized using a storm water sample. To eliminate chemical interference during the determination of silicon, graphite cuvettes have been modified with a permanent modifier (sodium tungstate) to form a carbide coating. The thermal stabilization of silicon in a graphite furnace has been achieved in the presence of a mixed palladium–magnesium modifier in the nitrate form. The developed method of analysis has been used to determine the content of polyorganosiloxanes (by silicon) in natural water samples. The metrological characteristics of the method in the determined silicon content range of 0.01–100 mg/dm3 have been estimated.

AB - A method for determination of polyorganosiloxanes (by silicon) in water using high-resolution continuum source electrothermal atomic absorption spectrometry with the preliminary extraction of the analytes from the analyzed sample by benzene is proposed. The parameters of the time–temperature program of an atomizer are optimized using a storm water sample. To eliminate chemical interference during the determination of silicon, graphite cuvettes have been modified with a permanent modifier (sodium tungstate) to form a carbide coating. The thermal stabilization of silicon in a graphite furnace has been achieved in the presence of a mixed palladium–magnesium modifier in the nitrate form. The developed method of analysis has been used to determine the content of polyorganosiloxanes (by silicon) in natural water samples. The metrological characteristics of the method in the determined silicon content range of 0.01–100 mg/dm3 have been estimated.

UR - http://www.scopus.com/inward/record.url?partnerID=8YFLogxK&scp=85188232716

UR - https://gateway.webofknowledge.com/gateway/Gateway.cgi?GWVersion=2&SrcAuth=tsmetrics&SrcApp=tsm_test&DestApp=WOS_CPL&DestLinkType=FullRecord&KeyUT=001187460500005

U2 - 10.1134/S0020168523140133

DO - 10.1134/S0020168523140133

M3 - Article

VL - 59

SP - 1387

EP - 1395

JO - Inorganic Materials

JF - Inorganic Materials

SN - 0020-1685

IS - 14

ER -

ID: 55300390